Ifeffit

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ifeffit@millenia.cars.aps.anl.gov

July 2003

15 participants
18 discussions

failure notice
by MAILER-DAEMON＠mail.hive.nj2.inquent.com 10 Jul '03

10 Jul '03

Hi. This is the qmail-send program at mail.hive.nj2.inquent.com. I'm afraid I wasn't able to deliver your message to the following addresses. This is a permanent error; I've given up. Sorry it didn't work out. <arnold(a)beryldshannon.com>: user is over quota --- Below this line is a copy of the message. Return-Path: <ifeffit(a)millenia.cars.aps.anl.gov> Received: (qmail 28325 invoked by uid 109); 10 Jul 2003 22:44:41 -0000 Delivered-To: beryldshannon.com-webmaster(a)beryldshannon.com Received: (qmail 28311 invoked from network); 10 Jul 2003 22:44:40 -0000 Received: from unknown (HELO COMPUTERNAME) (24.191.167.224) by 205.178.180.9 with SMTP; 10 Jul 2003 22:44:40 -0000 From: <ifeffit(a)millenia.cars.aps.anl.gov> To: <webmaster(a)beryldshannon.com> Subject: Re: Movie Date: Thu, 10 Jul 2003 18:44:40 --0400 Importance: Normal X-Mailer: Microsoft Outlook Express 6.00.2600.0000 X-MSMail-Priority: Normal X-Priority: 3 (Normal) MIME-Version: 1.0 Content-Type: multipart/mixed; boundary="CSmtpMsgPart123X456_000_00059887" This is a multipart message in MIME format --CSmtpMsgPart123X456_000_00059887 Content-Type: text/plain; charset="iso-8859-1" Content-Transfer-Encoding: 7bit Please see the attached zip file for details. --CSmtpMsgPart123X456_000_00059887 Content-Type: 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Using restraints in IFEFFIT
by Norbert Weiher 10 Jul '03

10 Jul '03

Hello, it's me again, it was a pleasure for me to hear that IFEFFIT can now handle restraints. I read the documentation on handling them on the IFEFFIT homepage but one thing is still unclear: I see how you can say that a value should be near some number you know from other methods. But how do I apply a range? Of course, I could always use the midpoint of the restraint interval and use the way described - but can you do it in other ways? The last question concerns the weighting factor: Let's keep with Matt's example of setting a restraint on a distance to 2.54. If I use the weighting of 0.01 shown in the example, what would be the max. and min. values the fit can run to? Is it +/- 1 % deviation or something else? Cheers, Norbert -- Dr. rer. nat. Norbert Weiher (norbertweiher(a)yahoo.de) Laboratory for Technical Chemistry - ETH Hönggerberg HCI E 117 - 8093 Zürich - Phone: +41 1 63 3 48 32

2 1

Virus Found in message "Application"
by Joe 10 Jul '03

10 Jul '03

Norton AntiVirus found a virus in an attachment you (ifeffit(a)millenia.cars.aps.anl.gov) sent to Joe. To ensure the recipient(s) are able to use the files you sent, perform a virus scan on your computer, clean any infected files, then resend this attachment. Attachment: your_details.zip Virus name: Multiple viruses found. Please see individual log messages. Action taken: Clean failed : Quarantine succeeded : File status: Still contains 1 infected items

1 0

Re: Ifeffit Digest, Vol 5, Issue 4
by Grant Bunker 09 Jul '03

09 Jul '03

In regard to global fitting, there are much better algorithms than a simple grid search, something we stared with the 70's. More recently I have had some good results with a very simple genetic algorithm called "differential evolution" by storn and price. It seems to be faster than simulated annealing, and it has the advantage of being very robust. It behaves well with hard constraints (e.g. integer programming) included by penalty functions (or if you like, terms incorporating a priori knowledge, from a bayesian point of view). It also looks to me like it would be trivial to parallelize for using multiple processors. I think the easiest thing to implement in feffit however would be simply to do a series of minimizations with (say, 1000) random starting points in the parameter space. This would just entail wrapping the minimization in a loop, and adding a way to summarize the results. Minimizations starting at differentpoints may end up in the same or different "attractors". If those corresponded to bad fits, throw them out. If they are adequate fits, keep them. Quite possibly more than one attractor could fit the data adequately. A cluster analysis of the results should indicate whether different solutions are equivalent (belong to the same attractor) or not. I don't think this should be very hard to do. Of course it easy to suggest that other people do the work, so I've been playing with these approaches myself using mathematica as my sandbox. The minimization code in feffit would have to be robust enough that it would give up gracefully (not crash) if it became numerically unstable. I think it should be fast enough that a global solution could be obtained in a couple of hours on a modern machine. If not, it could be done in an intrinsically parallel way on multiple machines. thanks - grant On Tue, 8 Jul 2003 ifeffit-request(a)millenia.cars.aps.anl.gov wrote: > Send Ifeffit mailing list submissions to > ifeffit(a)millenia.cars.aps.anl.gov > > To subscribe or unsubscribe via the World Wide Web, visit > http://millenia.cars.aps.anl.gov/mailman/listinfo/ifeffit > or, via email, send a message with subject or body 'help' to > ifeffit-request(a)millenia.cars.aps.anl.gov > > You can reach the person managing the list at > ifeffit-owner(a)millenia.cars.aps.anl.gov > > When replying, please edit your Subject line so it is more specific > than "Re: Contents of Ifeffit digest..." > > > Today's Topics: > > 1. Re: ARE: [Ifeffit] Re: Ifeffit Digest, Vol 5, Issue 1 > (Bruce Ravel) > 2. Re: Estimating error in XAS (Scott Calvin) > 3. Re: Re: Estimating error in XAS (Matt Newville) > 4. Re: Estimating error in XAS (Scott Calvin) > 5. Scanning of "Potential Surfaces" in EXAFS (Norbert Weiher) > 6. Re: Scanning of "Potential Surfaces" in EXAFS (Bruce Ravel) > > > ---------------------------------------------------------------------- > > Message: 1 > Date: Mon, 7 Jul 2003 13:11:08 -0400 > From: Bruce Ravel <ravel(a)phys.washington.edu> > Subject: Re: ARE: [Ifeffit] Re: Ifeffit Digest, Vol 5, Issue 1 > To: XAFS Analysis using Ifeffit <ifeffit(a)millenia.cars.aps.anl.gov> > Message-ID: <200307071311.08259.ravel(a)phys.washington.edu> > Content-Type: text/plain; charset="iso-8859-1" > > On Monday 07 July 2003 12:45 pm, Matt Newville wrote: > > Anyway, I think using the 'epsilon_k' that chi_noise() estimates as > > the noise in chi(k) is a fine way to do a weighted averages of data. > > It's not perfect, but neither is anything else. > > Exactly right! As Matt explained, there are reasons to believe that > the measurement uncertainty is dominated by things that Parsival's > theorem doesn't address and that measuring those problems is hard. > > As Matt said, weighting by 1/chi_noise() is OK. As Scott said, > weighting uniformly is OK. Those are two choices are the most OK I > can think of, so Athena will let you choose between them. > > While I am of the chorus of people agreeing with Grant that mu is not > equal to <If>/<I0>, I can see no reason why Athena should actively > prevent the user from looking at <If> or <I0>, if that is what he > wants to do. The *current* version of Athena prevents this, but > that's a bug not a feature! ;-) > > B > > > > -- > Bruce Ravel ----------------------------------- ravel(a)phys.washington.edu > Code 6134, Building 3, Room 222 > Naval Research Laboratory phone: (1) 202 767 5947 > Washington DC 20375, USA fax: (1) 202 767 1697 > > NRL Synchrotron Radiation Consortium (NRL-SRC) > Beamlines X11a, X11b, X23b, X24c, U4b > National Synchrotron Light Source > Brookhaven National Laboratory, Upton, NY 11973 > > My homepage: http://feff.phys.washington.edu/~ravel > EXAFS software: http://feff.phys.washington.edu/~ravel/software/exafs/ > > > ------------------------------ > > Message: 2 > Date: Mon, 7 Jul 2003 13:15:45 -0400 > From: Scott Calvin <scalvin(a)anvil.nrl.navy.mil> > Subject: [Ifeffit] Re: Estimating error in XAS > To: XAFS Analysis using Ifeffit <ifeffit(a)millenia.cars.aps.anl.gov> > Message-ID: <p05210602bb2f56d34214(a)[132.250.126.21]> > Content-Type: text/plain; charset="us-ascii" > > In the anecdotal category, I've seen some fairly bizarre high-r > behavior on beamline X23B at the NSLS, which I tentatively attribute > to feedback problems. That line, as many of you know, can be a little > pathological at times. I've also collected some data to examine this > issue on X11A, a more conventional beamline, but have never gotten > around to looking at it--I hope to soon. > > In any case, I don't really understand the logic of averaging scans > based on some estimate of the noise. For that to be appropriate, > you'd have to believe there was some systematic difference in the > noise between scans. What's causing that difference, if they're > collected on the same beamline on the same sample? (Or did I > misunderstand Michel's comment--was he talking about averaging data > from different beamlines or something?) If there is no systematic > changes during data collection, then the noise level should be the > same, and any attempt to weight by some proxy for the actual noise > will actually decrease the statistical content of the averaged data > by overweighting some scans (i. e. random fluctuations in the > quantity being used to estimate the uncertainty will cause some scans > to dominate the average more heavily, which is not ideal if the > actual noise level is the same). If, on the other hand, there is a > systematic difference between subsequent scans, it is fairly unlikely > to be "white," and thus will not be addressed by this scheme anyway. > Perhaps one of you can give me examples where this kind of variation > in data quality is found. > > So right now I don't see the benefit to this method. Particularly if > it's automated, I hesitate to add hidden complexity to my data > reduction without a clear rationale for it. > > --Scott Calvin > Naval Research Lab > Code 6344 > > Matt Newville wrote: > > > > >I'd assumed that vibrations would actually cause fairly white noise, > >though feedback mechanisms could skew towards high frequency. Other > >effects (temperature/pressure/flow fluctuations in ion chamber gases > >and optics) might skew toward low-frequency noises. I have not seen > >many studies of vibrations, feedback mechanism, or other > >beamline-specific effects on data quality, and none discussing the > >spectral weight of the beamline-specific noise. > > > >On the other hand, all data interpolation schemes do some smoothing, > >which suppresses high frequency components. And it usually appears > >that the high-frequency estimate of the noise from chi_noise() or > >Feffit gives an estimate that is significantly *low*. > > > >Anyway, I think using the 'epsilon_k' that chi_noise() estimates as > >the noise in chi(k) is a fine way to do a weighted averages of data. > >It's not perfect, but neither is anything else. > > > >--Matt > > > >_______________________________________________ > >Ifeffit mailing list > >Ifeffit(a)millenia.cars.aps.anl.gov > >http://millenia.cars.aps.anl.gov/mailman/listinfo/ifeffit >

4 3

ARE: [Ifeffit] Re: Ifeffit Digest, Vol 5, Issue 1
by SCHLEGEL Michel 177447 07 Jul '03

07 Jul '03

Hello everyone, > > I would second Matt's reservations about averaging I0 for > > different XAFS scans. The main reason we record I0 is to > > compensate for fluctuations in I0, which are mirrored in > > If (statistically they are highly correlated) so the ratio > > If/I0 eliminates the variation (as long as the > detector chain is linear). > I totally agree. This can lead to big problems in the data. We > accidentally tried it once and then made sure that the > <If/Io> average was performed instead. I think the best way to do it statistically is to weight each individual XAS spectrum with 1/s^2, where s is an estimate of the noise in the spectrum. This makes sure that a noisy spectrum does not alter the overall quality of the fit . Of course, a simpler way to do it is to retain only the spectra of overall similar -and hopefully good - quality, and discard the noisy ones. I think an evaluation of the spectrum noise may be obtained from the FT contributions peaking at high 'distances' (e.g., > 10Å). Hence, with a correct script, we should be able to: - extract chi(k) functions from individual XAS spectra - perform FTs for these spectra, - perform inverse FT on the spectra over a given limit, and calculate s from that, - usecalculated s values to sum weight-average individual XAS spectra. As I'm a very lousy IFEFFIT user (means that I've stopped short from hitting buttons on Athena and Artemis), I would humbly ask Bruce if there's any chance to see such a methodology implemented on Athena one of these days (not in a hurry, though) Best regards, Michel Schlegel

4 7

Re: Ifeffit Digest, Vol 5, Issue 1
by Grant Bunker 03 Jul '03

03 Jul '03

I would second Matt's reservations about averaging I0 for different XAFS scans. The main reason we record I0 is to compensate for fluctuations in I0, which are mirrored in If (statistically they are highly correlated) so the ratio If/I0 eliminates the variation (as long as the detector chain is linear). In short <If/I0> is not equal to <If>/<I0> where < > indicates the average. thanks - grant On Thu, 3 Jul 2003 ifeffit-request(a)millenia.cars.aps.anl.gov wrote: > Send Ifeffit mailing list submissions to > ifeffit(a)millenia.cars.aps.anl.gov > > To subscribe or unsubscribe via the World Wide Web, visit > http://millenia.cars.aps.anl.gov/mailman/listinfo/ifeffit > or, via email, send a message with subject or body 'help' to > ifeffit-request(a)millenia.cars.aps.anl.gov > > You can reach the person managing the list at > ifeffit-owner(a)millenia.cars.aps.anl.gov > > When replying, please edit your Subject line so it is more specific > than "Re: Contents of Ifeffit digest..." > > > Today's Topics: > > 1. Re: your mail (Matt Newville) > 2. merging I0 (Bruce Ravel) > > > ---------------------------------------------------------------------- > > Message: 1 > Date: Wed, 2 Jul 2003 16:20:47 -0500 (CDT) > From: Matt Newville <newville(a)cars.uchicago.edu> > Subject: [Ifeffit] Re: your mail > To: jshokes(a)sunchem.chem.uga.edu > Cc: XAFS Analysis using Ifeffit <ifeffit(a)millenia.cars.aps.anl.gov> > Message-ID: > <Pine.LNX.4.44.0307021605120.12464-100000(a)millenia.cars.aps.anl.gov> > Content-Type: TEXT/PLAIN; charset=US-ASCII > > Hi Jacob, > > Jacob Shokes (jshokes(a)chem.uga.edu) wrote: > > > I had a question I was hoping you could help me with. I have imported a > > bunch of ASCII type files into Athena and averaged them all together. The > > ASCII files contain the Energy, detector file, I0, I1, and I2. After I > > average the files together, I want to save the file and export it as an > > ASCII file. I understand how to do this, but when I do it I only obtain > > the Energy, [detector/IO], and background in column three (like it states > > in the manual). Now what I want to do, is extract the averaged I0 column > > from the process. Is there anyway to do this or will I just have to > > average I0 in another software. Any help with this would be appreciated. > > Sorry for the delay - I was away at the EXAFS conference, and am > still catching up on email. I hope it's OK that I forward this > question to the ifeffit mailing list, as others might have similar > questions, and Bruce Ravel might have a better answer. > > I believe you'd have to average all the I0 values yourself, and that > athena cannot do this easily. Bruce might correct me on this.... > It would be possible to do this using the Ifeffit commands directly > (including in the athena command window), something like this: > > read_data(mydat.001, group=a001, label='energy if i0') > read_data(mydat.002, group=a002, label='energy if i0') > read_data(mydat.003, group=a003, label='energy if i0') > ave.energy = (a001.energy + a002.energy + a003.energy ) / 3 > ave.if = (a001.if + a002.if + a003.if ) / 3 > ave.i0 = (a001.i0 + a002.i0 + a003.i0 ) / 3 > write_data(file= ave.dat, ave.energy, ave.if, ave.i0) > > In most cases I don't think you really want to do this, or use an > averaged I0 signal. For EXAFS data in transmission or fluorescence > (or electron yield), log(I0/I1) or IF/I0 can be averaged and merged, > but averaging I0 may not be meaningful. On the other hand, you might > be looking for typical I0 count rates, and the variations in I0, in > which case such averages might be useful. > > Hope that helps, > > --Matt > > > > > ------------------------------ > > Message: 2 > Date: Wed, 2 Jul 2003 17:55:43 -0400 > From: Bruce Ravel <ravel(a)phys.washington.edu> > Subject: [Ifeffit] merging I0 > To: XAFS Analysis using Ifeffit <ifeffit(a)millenia.cars.aps.anl.gov> > Cc: jshokes(a)sunchem.chem.uga.edu > Message-ID: <200307021755.43883.ravel(a)phys.washington.edu> > Content-Type: text/plain; charset="us-ascii" > > > Hi folks, > > As Matt suggested, I will take a stab at this question. > > > > I had a question I was hoping you could help me with. I have imported a > > > bunch of ASCII type files into Athena and averaged them all together. The > > > ASCII files contain the Energy, detector file, I0, I1, and I2. After I > > > average the files together, I want to save the file and export it as an > > > ASCII file. I understand how to do this, but when I do it I only obtain > > > the Energy, [detector/IO], and background in column three (like it states > > > in the manual). Now what I want to do, is extract the averaged I0 column > > > from the process. Is there anyway to do this or will I just have to > > > average I0 in another software. Any help with this would be appreciated. > > > I believe you'd have to average all the I0 values yourself, and that > > athena cannot do this easily. Bruce might correct me on this.... > > It would be possible to do this using the Ifeffit commands directly > > (including in the athena command window), something like this: > > Matt's suggeted sequence of raw ifeffit commands is certainly a fine > way of doing what Jacob asked for. Averaging I0 alone is not > something I had in mind when I designed Athena's basic interface > features, but it should be possible. > > As is the case when one tries to explain a sequence of mouse clicks, > this will be rather wordy. Sorry.... > > As all Athena users know, the first thing that happens when you import > a data file is to interact with the file selection dialog: > > http://leonardo.phys.washington.edu/~ravel/software/exafs/images/athena/col… > Athena remembers which columns were used to make the numerator and > denominator of the expression that constructs mu(E) from the column > data. (Note that the ability to make detector groups is lost once the > data are saved to a project file. Making detector groups is something > that must be done during the session in which the raw data are > imported.) > > In the Group menu is a option for "Make detector groups". This will > make entries in the Data groups list for the numerator and denominator > used to make the original data group. > > So my solution to Jacob's problem was to import data files one-by-one. > Each time, I made the detector groups. Once all the data was imported > and the detector groups were made, I marked the denominator groups (my > test data were all transmission, so I0 was in the denominator). Then, > in principle, one could select "Merge marked data in mu(E)" from the > Merge menu and have the merged I0 data that Jacob was looking for. > > *In principle*. In fact, there is a bug in the current version of > Athena and the merge of the I0 data failed. That bug will, however, > be fixed soon. Once that is done, it will be possible, albeit > inconvenient, to merge I0 data as Jacob wants. You may wish to try > working through the procedure that I described to understand how the > detector group feature of Athena works, even if the final step will > fail in the current version. > > B > > P.S. I am pretty certain that this will be fixed in time for the next > release of Athena and that the next release will be before Friday the > 11th. > > > -- > Bruce Ravel ----------------------------------- ravel(a)phys.washington.edu > Code 6134, Building 3, Room 222 > Naval Research Laboratory phone: (1) 202 767 5947 > Washington DC 20375, USA fax: (1) 202 767 1697 > > NRL Synchrotron Radiation Consortium (NRL-SRC) > Beamlines X11a, X11b, X23b, X24c, U4b > National Synchrotron Light Source > Brookhaven National Laboratory, Upton, NY 11973 > > My homepage: http://feff.phys.washington.edu/~ravel > EXAFS software: http://feff.phys.washington.edu/~ravel/software/exafs/ > > > ------------------------------ > > _______________________________________________ > Ifeffit mailing list > Ifeffit(a)millenia.cars.aps.anl.gov > http://millenia.cars.aps.anl.gov/mailman/listinfo/ifeffit > > > End of Ifeffit Digest, Vol 5, Issue 1 > ************************************* >

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merging I0
by Bruce Ravel 02 Jul '03

02 Jul '03

Hi folks, As Matt suggested, I will take a stab at this question. > > I had a question I was hoping you could help me with. I have imported a > > bunch of ASCII type files into Athena and averaged them all together. The > > ASCII files contain the Energy, detector file, I0, I1, and I2. After I > > average the files together, I want to save the file and export it as an > > ASCII file. I understand how to do this, but when I do it I only obtain > > the Energy, [detector/IO], and background in column three (like it states > > in the manual). Now what I want to do, is extract the averaged I0 column > > from the process. Is there anyway to do this or will I just have to > > average I0 in another software. Any help with this would be appreciated. > I believe you'd have to average all the I0 values yourself, and that > athena cannot do this easily. Bruce might correct me on this.... > It would be possible to do this using the Ifeffit commands directly > (including in the athena command window), something like this: Matt's suggeted sequence of raw ifeffit commands is certainly a fine way of doing what Jacob asked for. Averaging I0 alone is not something I had in mind when I designed Athena's basic interface features, but it should be possible. As is the case when one tries to explain a sequence of mouse clicks, this will be rather wordy. Sorry.... As all Athena users know, the first thing that happens when you import a data file is to interact with the file selection dialog: http://leonardo.phys.washington.edu/~ravel/software/exafs/images/athena/col… Athena remembers which columns were used to make the numerator and denominator of the expression that constructs mu(E) from the column data. (Note that the ability to make detector groups is lost once the data are saved to a project file. Making detector groups is something that must be done during the session in which the raw data are imported.) In the Group menu is a option for "Make detector groups". This will make entries in the Data groups list for the numerator and denominator used to make the original data group. So my solution to Jacob's problem was to import data files one-by-one. Each time, I made the detector groups. Once all the data was imported and the detector groups were made, I marked the denominator groups (my test data were all transmission, so I0 was in the denominator). Then, in principle, one could select "Merge marked data in mu(E)" from the Merge menu and have the merged I0 data that Jacob was looking for. *In principle*. In fact, there is a bug in the current version of Athena and the merge of the I0 data failed. That bug will, however, be fixed soon. Once that is done, it will be possible, albeit inconvenient, to merge I0 data as Jacob wants. You may wish to try working through the procedure that I described to understand how the detector group feature of Athena works, even if the final step will fail in the current version. B P.S. I am pretty certain that this will be fixed in time for the next release of Athena and that the next release will be before Friday the 11th. -- Bruce Ravel ----------------------------------- ravel(a)phys.washington.edu Code 6134, Building 3, Room 222 Naval Research Laboratory phone: (1) 202 767 5947 Washington DC 20375, USA fax: (1) 202 767 1697 NRL Synchrotron Radiation Consortium (NRL-SRC) Beamlines X11a, X11b, X23b, X24c, U4b National Synchrotron Light Source Brookhaven National Laboratory, Upton, NY 11973 My homepage: http://feff.phys.washington.edu/~ravel EXAFS software: http://feff.phys.washington.edu/~ravel/software/exafs/

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Re: your mail
by Matt Newville 02 Jul '03

02 Jul '03

Hi Jacob, Jacob Shokes (jshokes(a)chem.uga.edu) wrote: > I had a question I was hoping you could help me with. I have imported a > bunch of ASCII type files into Athena and averaged them all together. The > ASCII files contain the Energy, detector file, I0, I1, and I2. After I > average the files together, I want to save the file and export it as an > ASCII file. I understand how to do this, but when I do it I only obtain > the Energy, [detector/IO], and background in column three (like it states > in the manual). Now what I want to do, is extract the averaged I0 column > from the process. Is there anyway to do this or will I just have to > average I0 in another software. Any help with this would be appreciated. Sorry for the delay - I was away at the EXAFS conference, and am still catching up on email. I hope it's OK that I forward this question to the ifeffit mailing list, as others might have similar questions, and Bruce Ravel might have a better answer. I believe you'd have to average all the I0 values yourself, and that athena cannot do this easily. Bruce might correct me on this.... It would be possible to do this using the Ifeffit commands directly (including in the athena command window), something like this: read_data(mydat.001, group=a001, label='energy if i0') read_data(mydat.002, group=a002, label='energy if i0') read_data(mydat.003, group=a003, label='energy if i0') ave.energy = (a001.energy + a002.energy + a003.energy ) / 3 ave.if = (a001.if + a002.if + a003.if ) / 3 ave.i0 = (a001.i0 + a002.i0 + a003.i0 ) / 3 write_data(file= ave.dat, ave.energy, ave.if, ave.i0) In most cases I don't think you really want to do this, or use an averaged I0 signal. For EXAFS data in transmission or fluorescence (or electron yield), log(I0/I1) or IF/I0 can be averaged and merged, but averaging I0 may not be meaningful. On the other hand, you might be looking for typical I0 count rates, and the variations in I0, in which case such averages might be useful. Hope that helps, --Matt

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