Two analysts, one spectrum, similar outcome?
Hi Everyone, I'm curious, has anyone ever tried turning two analysts loose on the same unknown EXAFS spectrum to see if their fits come out with similar conclusions? If you have tried it, how did it work out? Were the conclusions indeed similar? If not, why not, and what did you end up doing about it? I was talking with a colleague today about our plans for data analysis, and we settled on this approach (since there are two interested parties willing to try to fit a series of unknown EXAFS datasets). The hope is, of course, that the two analysts will independently reach similar conclusions with similar fits and structural models, but to my mind that outcome is by no means guaranteed. Given the (presumably) wide variation in fitting customs and procedures, I can envision a scenario in which there are major differences. This got me wondering, "Has anyone tried this?" So I thought I'd ask. Your thoughts and experiences would be welcome. Thanks! Mike Massey
Are they equally smart? Anatoly
On Aug 13, 2019, at 9:39 PM, Mike Massey
wrote: Hi Everyone,
I'm curious, has anyone ever tried turning two analysts loose on the same unknown EXAFS spectrum to see if their fits come out with similar conclusions? If you have tried it, how did it work out? Were the conclusions indeed similar? If not, why not, and what did you end up doing about it?
I was talking with a colleague today about our plans for data analysis, and we settled on this approach (since there are two interested parties willing to try to fit a series of unknown EXAFS datasets).
The hope is, of course, that the two analysts will independently reach similar conclusions with similar fits and structural models, but to my mind that outcome is by no means guaranteed. Given the (presumably) wide variation in fitting customs and procedures, I can envision a scenario in which there are major differences.
This got me wondering, "Has anyone tried this?" So I thought I'd ask.
Your thoughts and experiences would be welcome. Thanks!
Mike Massey _______________________________________________ Ifeffit mailing list Ifeffit@millenia.cars.aps.anl.gov http://millenia.cars.aps.anl.gov/mailman/listinfo/ifeffit Unsubscribe: http://millenia.cars.aps.anl.gov/mailman/options/ifeffit
I'm the dumb one. But it's an interesting question, and gets perhaps to the heart of the issue: to what extent does the smartness of the analyst, or their experience, or the fitting procedures used, or a butterfly flapping its wings in Micronesia, impact the results? For the sake of argument, can two equally smart and experienced analysts working on fitting the same EXAFS spectra be expected to reach similar conclusions? I guess we'll find out. Another colleague once said something like, "EXAFS is great: you publish a paper, then later you publish another paper re-analyzing the same data." Of course, he's a strictly computational guy, so I'm not sure he necessarily has standing to criticize...(Good-natured sarcasm font...)
On Aug 13, 2019, at 6:43 PM, Anatoly Frenkel
wrote: Are they equally smart?
Anatoly
On Aug 13, 2019, at 9:39 PM, Mike Massey
wrote: Hi Everyone,
I'm curious, has anyone ever tried turning two analysts loose on the same unknown EXAFS spectrum to see if their fits come out with similar conclusions? If you have tried it, how did it work out? Were the conclusions indeed similar? If not, why not, and what did you end up doing about it?
I was talking with a colleague today about our plans for data analysis, and we settled on this approach (since there are two interested parties willing to try to fit a series of unknown EXAFS datasets).
The hope is, of course, that the two analysts will independently reach similar conclusions with similar fits and structural models, but to my mind that outcome is by no means guaranteed. Given the (presumably) wide variation in fitting customs and procedures, I can envision a scenario in which there are major differences.
This got me wondering, "Has anyone tried this?" So I thought I'd ask.
Your thoughts and experiences would be welcome. Thanks!
Mike Massey _______________________________________________ Ifeffit mailing list Ifeffit@millenia.cars.aps.anl.gov http://millenia.cars.aps.anl.gov/mailman/listinfo/ifeffit Unsubscribe: http://millenia.cars.aps.anl.gov/mailman/options/ifeffit
_______________________________________________ Ifeffit mailing list Ifeffit@millenia.cars.aps.anl.gov http://millenia.cars.aps.anl.gov/mailman/listinfo/ifeffit Unsubscribe: http://millenia.cars.aps.anl.gov/mailman/options/ifeffit
The answer you get will depend somewhat on the assumptions you make. if you are truly provided with data and no other information about the sample, then the job is challenging. If you know something about the sample that can help you start in a particular direction then the two analyses have a better chance of converging but it still depends on how you decide to approach the structural model. You also need to think about what question you are trying to answer. If you have a specific goal in mind, then you may choose a different model than the individual who is seeking the answer to a different question. The most likely way to approach this problem is to both have the same background information about the sample(s) and to mutually determine what question you are trying to answer. Cheers, Carlo On Tue, 13 Aug 2019, Mike Massey wrote:
I'm the dumb one. But it's an interesting question, and gets perhaps to the heart of the issue: to what extent does the smartness of the analyst, or their experience, or the fitting procedures used, or a butterfly flapping its wings in Micronesia, impact the results?
For the sake of argument, can two equally smart and experienced analysts working on fitting the same EXAFS spectra be expected to reach similar conclusions? I guess we'll find out.
Another colleague once said something like, "EXAFS is great: you publish a paper, then later you publish another paper re-analyzing the same data." Of course, he's a strictly computational guy, so I'm not sure he necessarily has standing to criticize...(Good-natured sarcasm font...)
On Aug 13, 2019, at 6:43 PM, Anatoly Frenkel
wrote: Are they equally smart?
Anatoly
On Aug 13, 2019, at 9:39 PM, Mike Massey
wrote: Hi Everyone,
I'm curious, has anyone ever tried turning two analysts loose on the same unknown EXAFS spectrum to see if their fits come out with similar conclusions? If you have tried it, how did it work out? Were the conclusions indeed similar? If not, why not, and what did you end up doing about it?
I was talking with a colleague today about our plans for data analysis, and we settled on this approach (since there are two interested parties willing to try to fit a series of unknown EXAFS datasets).
The hope is, of course, that the two analysts will independently reach similar conclusions with similar fits and structural models, but to my mind that outcome is by no means guaranteed. Given the (presumably) wide variation in fitting customs and procedures, I can envision a scenario in which there are major differences.
This got me wondering, "Has anyone tried this?" So I thought I'd ask.
Your thoughts and experiences would be welcome. Thanks!
Mike Massey _______________________________________________ Ifeffit mailing list Ifeffit@millenia.cars.aps.anl.gov http://millenia.cars.aps.anl.gov/mailman/listinfo/ifeffit Unsubscribe: http://millenia.cars.aps.anl.gov/mailman/options/ifeffit
_______________________________________________ Ifeffit mailing list Ifeffit@millenia.cars.aps.anl.gov http://millenia.cars.aps.anl.gov/mailman/listinfo/ifeffit Unsubscribe: http://millenia.cars.aps.anl.gov/mailman/options/ifeffit
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-- Carlo U. Segre -- Duchossois Leadership Professor of Physics Directory, Center for Synchrotron Radiation Research and Instrumentation Illinois Institute of Technology Voice: 312.567.3498 Fax: 312.567.3494 segre@iit.edu http://phys.iit.edu/~segre segre@debian.org
It is true that we both have background information regarding the samples, and similar goals in terms of the questions we are looking to answer. "You also need to think about what question you are trying to answer. If you have a specific goal in mind, then you may choose a different model than the individual who is seeking the answer to a different question." This is, somewhat, the issue we are grappling with. A reasonable EXAFS fit is one interpretation of the data, but we are trying to find a way to deal with the problem of seeing what one wants to see in EXAFS data. To me, it's a bit of a problem, anyway. A version of "confirmation bias," I suppose. The hope is that, if two of us independently reach a similar conclusion, we can have more confidence in the findings, perhaps?
On Aug 13, 2019, at 7:59 PM, Carlo Segre
wrote: The answer you get will depend somewhat on the assumptions you make. if you are truly provided with data and no other information about the sample, then the job is challenging. If you know something about the sample that can help you start in a particular direction then the two analyses have a better chance of converging but it still depends on how you decide to approach the structural model.
You also need to think about what question you are trying to answer. If you have a specific goal in mind, then you may choose a different model than the individual who is seeking the answer to a different question.
The most likely way to approach this problem is to both have the same background information about the sample(s) and to mutually determine what question you are trying to answer.
Cheers,
Carlo
On Tue, 13 Aug 2019, Mike Massey wrote:
I'm the dumb one. But it's an interesting question, and gets perhaps to the heart of the issue: to what extent does the smartness of the analyst, or their experience, or the fitting procedures used, or a butterfly flapping its wings in Micronesia, impact the results?
For the sake of argument, can two equally smart and experienced analysts working on fitting the same EXAFS spectra be expected to reach similar conclusions? I guess we'll find out.
Another colleague once said something like, "EXAFS is great: you publish a paper, then later you publish another paper re-analyzing the same data." Of course, he's a strictly computational guy, so I'm not sure he necessarily has standing to criticize...(Good-natured sarcasm font...)
On Aug 13, 2019, at 6:43 PM, Anatoly Frenkel
wrote: Are they equally smart?
Anatoly
On Aug 13, 2019, at 9:39 PM, Mike Massey
wrote: Hi Everyone,
I'm curious, has anyone ever tried turning two analysts loose on the same unknown EXAFS spectrum to see if their fits come out with similar conclusions? If you have tried it, how did it work out? Were the conclusions indeed similar? If not, why not, and what did you end up doing about it?
I was talking with a colleague today about our plans for data analysis, and we settled on this approach (since there are two interested parties willing to try to fit a series of unknown EXAFS datasets).
The hope is, of course, that the two analysts will independently reach similar conclusions with similar fits and structural models, but to my mind that outcome is by no means guaranteed. Given the (presumably) wide variation in fitting customs and procedures, I can envision a scenario in which there are major differences.
This got me wondering, "Has anyone tried this?" So I thought I'd ask.
Your thoughts and experiences would be welcome. Thanks!
Mike Massey _______________________________________________ Ifeffit mailing list Ifeffit@millenia.cars.aps.anl.gov http://millenia.cars.aps.anl.gov/mailman/listinfo/ifeffit Unsubscribe: http://millenia.cars.aps.anl.gov/mailman/options/ifeffit
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-- Carlo U. Segre -- Duchossois Leadership Professor of Physics Directory, Center for Synchrotron Radiation Research and Instrumentation Illinois Institute of Technology Voice: 312.567.3498 Fax: 312.567.3494 segre@iit.edu http://phys.iit.edu/~segre segre@debian.org _______________________________________________ Ifeffit mailing list Ifeffit@millenia.cars.aps.anl.gov http://millenia.cars.aps.anl.gov/mailman/listinfo/ifeffit Unsubscribe: http://millenia.cars.aps.anl.gov/mailman/options/ifeffit
Hi Mike: What I mean by "what question you are trying to answer" is that if you are interested in a specific fitting parameter, you might wish to make some assumptions and put constraints on other parameters so that you can extract the trend that you are interested in. Carlo On Tue, 13 Aug 2019, Mike Massey wrote:
It is true that we both have background information regarding the samples, and similar goals in terms of the questions we are looking to answer.
"You also need to think about what question you are trying to answer. If you have a specific goal in mind, then you may choose a different model than the individual who is seeking the answer to a different question."
This is, somewhat, the issue we are grappling with. A reasonable EXAFS fit is one interpretation of the data, but we are trying to find a way to deal with the problem of seeing what one wants to see in EXAFS data. To me, it's a bit of a problem, anyway. A version of "confirmation bias," I suppose.
The hope is that, if two of us independently reach a similar conclusion, we can have more confidence in the findings, perhaps?
On Aug 13, 2019, at 7:59 PM, Carlo Segre
wrote: The answer you get will depend somewhat on the assumptions you make. if you are truly provided with data and no other information about the sample, then the job is challenging. If you know something about the sample that can help you start in a particular direction then the two analyses have a better chance of converging but it still depends on how you decide to approach the structural model.
You also need to think about what question you are trying to answer. If you have a specific goal in mind, then you may choose a different model than the individual who is seeking the answer to a different question.
The most likely way to approach this problem is to both have the same background information about the sample(s) and to mutually determine what question you are trying to answer.
Cheers,
Carlo
On Tue, 13 Aug 2019, Mike Massey wrote:
I'm the dumb one. But it's an interesting question, and gets perhaps to the heart of the issue: to what extent does the smartness of the analyst, or their experience, or the fitting procedures used, or a butterfly flapping its wings in Micronesia, impact the results?
For the sake of argument, can two equally smart and experienced analysts working on fitting the same EXAFS spectra be expected to reach similar conclusions? I guess we'll find out.
Another colleague once said something like, "EXAFS is great: you publish a paper, then later you publish another paper re-analyzing the same data." Of course, he's a strictly computational guy, so I'm not sure he necessarily has standing to criticize...(Good-natured sarcasm font...)
On Aug 13, 2019, at 6:43 PM, Anatoly Frenkel
wrote: Are they equally smart?
Anatoly
On Aug 13, 2019, at 9:39 PM, Mike Massey
wrote: Hi Everyone,
I'm curious, has anyone ever tried turning two analysts loose on the same unknown EXAFS spectrum to see if their fits come out with similar conclusions? If you have tried it, how did it work out? Were the conclusions indeed similar? If not, why not, and what did you end up doing about it?
I was talking with a colleague today about our plans for data analysis, and we settled on this approach (since there are two interested parties willing to try to fit a series of unknown EXAFS datasets).
The hope is, of course, that the two analysts will independently reach similar conclusions with similar fits and structural models, but to my mind that outcome is by no means guaranteed. Given the (presumably) wide variation in fitting customs and procedures, I can envision a scenario in which there are major differences.
This got me wondering, "Has anyone tried this?" So I thought I'd ask.
Your thoughts and experiences would be welcome. Thanks!
Mike Massey _______________________________________________ Ifeffit mailing list Ifeffit@millenia.cars.aps.anl.gov http://millenia.cars.aps.anl.gov/mailman/listinfo/ifeffit Unsubscribe: http://millenia.cars.aps.anl.gov/mailman/options/ifeffit
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-- Carlo U. Segre -- Duchossois Leadership Professor of Physics Directory, Center for Synchrotron Radiation Research and Instrumentation Illinois Institute of Technology Voice: 312.567.3498 Fax: 312.567.3494 segre@iit.edu http://phys.iit.edu/~segre segre@debian.org _______________________________________________ Ifeffit mailing list Ifeffit@millenia.cars.aps.anl.gov http://millenia.cars.aps.anl.gov/mailman/listinfo/ifeffit Unsubscribe: http://millenia.cars.aps.anl.gov/mailman/options/ifeffit
-- Carlo U. Segre -- Duchossois Leadership Professor of Physics Directory, Center for Synchrotron Radiation Research and Instrumentation Illinois Institute of Technology Voice: 312.567.3498 Fax: 312.567.3494 segre@iit.edu http://phys.iit.edu/~segre segre@debian.org
Dear Carlo. Regarding yours of Tue, 13 Aug 2019 21:59:18 -0500 (CDT): The way I like to put it is that EXAFS works best if you already know most of the answer. You need to have a specific question, such as 'is there antisite disorder?' or 'Are there edge-sharing octahedra?', or 'Which of three structures does this most resemble?'. I love the idea of blind analysis comparison. Sincerely, Matthew Marcus
The answer you get will depend somewhat on the assumptions you make. if you are truly provided with data and no other information about the sample, then the job is challenging. If you know something about the sample that can help you start in a particular direction then the two analyses have a better chance of converging but it still depends on how you decide to approach the structural model.
You also need to think about what question you are trying to answer. If you have a specific goal in mind, then you may choose a different model than the individual who is seeking the answer to a different question.
The most likely way to approach this problem is to both have the same background information about the sample(s) and to mutually determine what question you are trying to answer.
Cheers,
Carlo
On Tue, 13 Aug 2019, Mike Massey wrote:
I'm the dumb one. But it's an interesting question, and gets perhaps to the heart of the issue: to what extent does the smartness of the analyst, or their experience, or the fitting procedures used, or a butterfly flapping its wings in Micronesia, impact the results?
For the sake of argument, can two equally smart and experienced analysts working on fitting the same EXAFS spectra be expected to reach similar conclusions? I guess we'll find out.
Another colleague once said something like, "EXAFS is great: you publish a paper, then later you publish another paper re-analyzing the same data." Of course, he's a strictly computational guy, so I'm not sure he necessarily has standing to criticize...(Good-natured sarcasm font...)
On Aug 13, 2019, at 6:43 PM, Anatoly Frenkel
wrote: Are they equally smart?
Anatoly
On Aug 13, 2019, at 9:39 PM, Mike Massey
wrote: Hi Everyone,
I'm curious, has anyone ever tried turning two analysts loose on the same unknown EXAFS spectrum to see if their fits come out with similar conclusions? If you have tried it, how did it work out? Were the conclusions indeed similar? If not, why not, and what did you end up doing about it?
I was talking with a colleague today about our plans for data analysis, and we settled on this approach (since there are two interested parties willing to try to fit a series of unknown EXAFS datasets).
The hope is, of course, that the two analysts will independently reach similar conclusions with similar fits and structural models, but to my mind that outcome is by no means guaranteed. Given the (presumably) wide variation in fitting customs and procedures, I can envision a scenario in which there are major differences.
This got me wondering, "Has anyone tried this?" So I thought I'd ask.
Your thoughts and experiences would be welcome. Thanks!
Mike Massey _______________________________________________ Ifeffit mailing list Ifeffit@millenia.cars.aps.anl.gov http://millenia.cars.aps.anl.gov/mailman/listinfo/ifeffit Unsubscribe: http://millenia.cars.aps.anl.gov/mailman/options/ifeffit
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Yes, I did.
I set up a double-blind experiment with mixtures of various iron standards
and an “unknown” iron-containing compound. This was years ago, so I may
have a few details wrong, but it will get the gist:
I used undergraduates to make the mixtures with random amounts of random
selections of the standards. An undergraduate also ordered the “unknown”
compound.
We then measured the spectra, along with the spectra of the pure standards
(but not the pure “unknown”). The spectra were measured at somewhat
different temperatures so that simple linear combination analysis would be
of limited use. Three of us then attempted analysis independently: myself,
one of my most advanced undergraduates (who did not participate in the
preparation of the samples), and a high school student with roughly two
weeks training in analysis. We attempted to find what compounds were
present, how much of each, and, in the case of the unknown compound, as
much as we could suss out structurally.
The results were that we all did OK, but my analyses were the most
accurate, the advanced undergraduate less so, and the high school student
the least (but still generally in the ballpark).
It was satisfying to know that different analysts could find similar
results, that those results reflected reality, and that those with greater
expertise did achieve more accurate results.
If I recall correctly, I didn’t publish because the undergraduate who
prepared the pure standards did a lousy job (pinholes, etc.), which
distorted our measurement of the standards enough to make it more difficult
to evaluate our analyses. Still, it showed things work in principle.
The data, including a remeasured set of standards, is still available as
the EXAFS Divination Set http://xafs.org/EXAFS_Divination_Set.
Best,
Scott Calvin
Lehman College of the City University of New York
On Tue, Aug 13, 2019 at 9:41 PM Mike Massey
Hi Everyone,
I'm curious, has anyone ever tried turning two analysts loose on the same unknown EXAFS spectrum to see if their fits come out with similar conclusions? If you have tried it, how did it work out? Were the conclusions indeed similar? If not, why not, and what did you end up doing about it?
I was talking with a colleague today about our plans for data analysis, and we settled on this approach (since there are two interested parties willing to try to fit a series of unknown EXAFS datasets).
The hope is, of course, that the two analysts will independently reach similar conclusions with similar fits and structural models, but to my mind that outcome is by no means guaranteed. Given the (presumably) wide variation in fitting customs and procedures, I can envision a scenario in which there are major differences.
This got me wondering, "Has anyone tried this?" So I thought I'd ask.
Your thoughts and experiences would be welcome. Thanks!
Mike Massey _______________________________________________ Ifeffit mailing list Ifeffit@millenia.cars.aps.anl.gov http://millenia.cars.aps.anl.gov/mailman/listinfo/ifeffit Unsubscribe: http://millenia.cars.aps.anl.gov/mailman/options/ifeffit
This is a great example, Scott! Thanks for sharing your experience. Hopefully ours will be similarly positive and the results will be in the ballpark of each other. It's at least comforting to know there's a chance. Mike
On Aug 13, 2019, at 8:18 PM, Scott Calvin
wrote: Yes, I did.
I set up a double-blind experiment with mixtures of various iron standards and an “unknown” iron-containing compound. This was years ago, so I may have a few details wrong, but it will get the gist:
I used undergraduates to make the mixtures with random amounts of random selections of the standards. An undergraduate also ordered the “unknown” compound.
We then measured the spectra, along with the spectra of the pure standards (but not the pure “unknown”). The spectra were measured at somewhat different temperatures so that simple linear combination analysis would be of limited use. Three of us then attempted analysis independently: myself, one of my most advanced undergraduates (who did not participate in the preparation of the samples), and a high school student with roughly two weeks training in analysis. We attempted to find what compounds were present, how much of each, and, in the case of the unknown compound, as much as we could suss out structurally.
The results were that we all did OK, but my analyses were the most accurate, the advanced undergraduate less so, and the high school student the least (but still generally in the ballpark).
It was satisfying to know that different analysts could find similar results, that those results reflected reality, and that those with greater expertise did achieve more accurate results.
If I recall correctly, I didn’t publish because the undergraduate who prepared the pure standards did a lousy job (pinholes, etc.), which distorted our measurement of the standards enough to make it more difficult to evaluate our analyses. Still, it showed things work in principle.
The data, including a remeasured set of standards, is still available as the EXAFS Divination Set.
Best,
Scott Calvin Lehman College of the City University of New York
On Tue, Aug 13, 2019 at 9:41 PM Mike Massey
wrote: Hi Everyone, I'm curious, has anyone ever tried turning two analysts loose on the same unknown EXAFS spectrum to see if their fits come out with similar conclusions? If you have tried it, how did it work out? Were the conclusions indeed similar? If not, why not, and what did you end up doing about it?
I was talking with a colleague today about our plans for data analysis, and we settled on this approach (since there are two interested parties willing to try to fit a series of unknown EXAFS datasets).
The hope is, of course, that the two analysts will independently reach similar conclusions with similar fits and structural models, but to my mind that outcome is by no means guaranteed. Given the (presumably) wide variation in fitting customs and procedures, I can envision a scenario in which there are major differences.
This got me wondering, "Has anyone tried this?" So I thought I'd ask.
Your thoughts and experiences would be welcome. Thanks!
Mike Massey _______________________________________________ Ifeffit mailing list Ifeffit@millenia.cars.aps.anl.gov http://millenia.cars.aps.anl.gov/mailman/listinfo/ifeffit Unsubscribe: http://millenia.cars.aps.anl.gov/mailman/options/ifeffit
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participants (5)
-
Anatoly Frenkel
-
Carlo Segre
-
Matthew Marcus
-
Mike Massey
-
Scott Calvin