[Ifeffit] Fe K edge spectrum of scorodite

Case Van Genuchten cmvangenuchten at gmail.com
Mon Jul 6 11:12:21 CDT 2015


Dear Matthew,

Sure, the raw data and/or spectrum can be added to the database.  For this
sample, the 1st derivative of the Fe foil was 7.112 keV.  I can also
provide individual scans for the database, if needed.  Is there any
interest in the As K-edge of this sample, too?  I have that one as well.
Case

On Mon, Jul 6, 2015 at 5:48 PM, Matthew Marcus <mamarcus at lbl.gov> wrote:

> Thanks!  May I add it to the ALS 10.3.2 reference collection?
>
> What is the standard of energy calibration?  Is the Fe metal edge at
> 7110.75eV, 7112eV or what?
>         mam
>
> On 7/6/2015 7:11 AM, Case Van Genuchten wrote:
>
>> Dear Shaofeng,
>>
>> I am attaching the averaged, raw data and Fe K-edge EXAFS spectrum
>> (extracted using SixPack) of scorodite.  The mineral was prepared following
>> the procedure outlined in Paktunc et al. (2008).  The data were collected
>> at the Stanford Synchrotron Radiation Lightsource in transmission mode with
>> the sample housed in a liquid nitrogen cryostat.  You can find additional
>> details on the preparation of the sample and data collection from the
>> publication where the spectrum is reported and modeled (van Genuchten et
>> al. 2014, Geochimica et Cosmochimica Acta).
>>
>> Please let me know if you have any other questions about data collection.
>>
>> Best,
>>
>> Case M. van Genuchten
>> Environmental Geochemistry Laboratory
>> Institute of Earth Surface Dynamics
>> University of Lausanne, Lausanne, CH
>>
>>
>>
>> On Mon, Jul 6, 2015 at 4:02 AM, Shaofeng Wang <wangshaofeng at iae.ac.cn
>> <mailto:wangshaofeng at iae.ac.cn>> wrote:
>>
>>     Dear all,
>>     Can anyone have Fe K edge exafs spectrum of scorodite share a copy?
>>     Thanks in advance.
>>     Shaofeng
>>     --------------------------------------
>>     Shaofeng Wang, Ph.D of Geochemistry
>>     Environmental Molecular Science Group
>>     Institute of Applied Ecology, Chinese Academy of Sciences
>>     Shenyang, 110016, China
>>     wangshaofeng at iae.ac.cn <mailto:wangshaofeng at iae.ac.cn>
>>     www.iae.cas.cn <http://www.iae.cas.cn>
>>
>>
>>
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