Hi everyone,
I doing LCF on my XANES data. I wonder if someone can tell me the
meaning of the values in parentheses following the weight value in
the Fit results window?. I looked into the respective document
section of the Manuel but could not find the answer, yet.
I am asking because I did a Fitting with over 20 standards (STD) to
find all combination of max 4 standards which describe my unknown
sample spectra. This results in a lot of combination with similar
chi-square(reduced) and R-values. I know a relative changes between
these values are more probably meaningful than absolute values.
A lot of the possible combinations provided by after the fit yieled
combinations with at lest on STD having a weight of 0.000. (Fit 1).
I thought that this would mean, that 3 standards are sufficient to
describe the system. However, repeating the fit with only the three
standards with weight > 0.0 yielded a complete different
proportions (Fit 2). How can this be explain and how should I deal
with combinations or standards having a weight of 0.000?
Thanks a lot for your thoughts and suggesting,
Cheers Paul
Results Fit 1:
3: STD3 0.324(0.025)
7: STD7 0.686(0.021)
20: STD2O 0.127(0.016)
27: STD27 0.000(0.036)
vs.
Results Fit 2:
3: STD3 0.473(0.019)
7: STD7 0.620(0.023)
20: STD20 0.000(0.030)