Dear Sir or Madam,
I got a normalized Fe K-edge EXAFS spectrum for my amorphous
7-component alloy
sample, for which I know its atomic percent composition.
I need to find out the interatomic distances between the Fe and
the other atoms
present in the alloy (identify the peaks in R-space) as well as
how many
atoms of each element is surrounding the absorbing iron atom
(coordination
number).
To meet my goal, I
think I need to fit the R-space Fourier transform of my EXAFS
spectrum in a
program like Artemis. Unfortunately, I haven`t found any
tutorial discussing
how to deal with amorphous sample with unknown organization of
the atoms. When
you are about to prepare an atomic model in Artemis for fitting,
you need to
build a model with an initial interatomic distances, atomic
coordination number,
etc, but all that is obviously unknown to me. I know nothing
about the short
range order in my material and I want to learn it from the
experiment itself (note
that it can be and most
probably is
different from the one present in crystalline structures). So,
my question is,
could somebody tell me how to deal with such system using the
Artemis, what
type of initial models for fitting should be prepared?
All of your help will be greatly appreciated.
Best regards,
Piotr Bardziński,